涓€銆佺櫧閰掍腑鐢查唶妾㈡脯(c猫)鍒嗘瀽鍘熺悊锛�
鎸夌収銆婇鍝佷腑鐢查唶鐨勬脯(c猫)瀹氥€嬭捀椁鹃櫎鍘荤櫦(f膩)閰甸厭鍙婂叾閰嶅埗閰掍腑涓嶆彯鐧�(f膩)鎬х墿璩�(zh矛),鍔犲叆鍏�(n猫i)妯�(bi膩o)(閰掔簿銆佽捀椁鹃厭鍙婂叾閰嶅埗閰掔洿鎺ュ姞鍏ュ収(n猫i)妯�(bi膩o)),缍�(j墨ng)姘ｇ浉鑹茶瓬鍎€鑹茶瓬鏌卞垎闆�,姘伀鐒伴洟瀛愬寲妾㈡脯(c猫)鍣ㄦ娓�(c猫),浠ヤ繚鐣欐檪(sh铆)闁撳畾鎬�,鍏�(n猫i)妯�(bi膩o)娉曞畾閲�
浜�銆佺櫧閰掍腑鐢查唶妾㈡脯(c猫)鍎€鍣ㄥ強妯�(bi膩o)婧�(zh菙n)鍝�
GC-9860姘ｇ浉鑹茶瓬鍎€锛團ID姘伀鐒版娓�(c猫)鍣�+姣涚窗(x矛)绠＄郴绲�(t菕ng)+鍏礆(j铆)绋嬪崌锛� 1鑷�(t谩i)
鐧介厭鍒嗘瀽灏�(zhu膩n)鐢ㄦ煴锛圥EG姣涚窗(x矛)绠℃煴60绫筹級 1鏀�
鑹茶瓬宸ヤ綔绔� 1濂�
绌烘埃銆佹爱?d煤)?銆佹矮姘ｇ櫦(f膩)鐢熷櫒鎴栭嫾鐡� 1濂�1路 1
闆昏叇鎵撳嵃姗�(j墨)鑷厤 1鑷�(t谩i)
妯�(bi膩o)婧�(zh菙n)鍝�
涔欓唶婧舵恫(40%,楂旂⿳鍒�?j菒n)?sh霉)):閲忓彇40mL涔欓唶,鐢ㄦ按瀹氬鑷�100mL,娣峰嫽銆�
鐢查唶(CH4O,CAS铏�(h脿o):67-56-1):绱斿害鈮�99%銆傛垨缍�(j墨ng)鍦�(gu贸)瀹惰獚(r猫n)璀夊苟鎺堜簣妯�(bi膩o)婧�(zh菙n)鐗╄唱(zh矛)璀夋浉(sh奴)鐨勬(bi膩o)婧�(zh菙n)鐗╄唱(zh矛)銆�
鍙旀垔閱�(C5H12O,CAS铏�(h脿o):75-85-4):绱斿害鈮�99%銆�
涓�銆佺櫧閰掍腑鐢查唶妾㈡脯(c猫)鍎€鍣ㄦ(bi膩o)婧�(zh菙n)婧舵恫閰嶅埗
鐢查唶妯�(bi膩o)婧�(zh菙n)鍎�(ch菙)鍌欐恫(5000mg/L):婧�(zh菙n)纰虹ū(ch膿ng)鍙�0.5g(**鑷�0.001g)鐢查唶鑷�100mL瀹归噺鐡朵腑,鐢ㄤ箼閱囨憾娑插畾瀹硅嚦鍒诲害,娣峰嫽,0鈩儈4鈩冧綆婧啺绠卞瘑灏佷繚瀛�銆�
鍙旀垔閱囨(bi膩o)婧�(zh菙n)婧舵恫(20000mg/L):婧�(zh菙n)纰虹ū(ch膿ng)鍙�2.0g(**鑷�0.001g)鍙旀垔閱囪嚦100mL瀹归噺鐡朵腑,鐢ㄤ箼閱囨憾娑插畾瀹硅嚦100mL,娣峰嫽,0鈩儈4鈩冧綆婧啺绠卞瘑灏佷繚瀛�銆�
鐢查唶绯诲垪妯�(bi膩o)婧�(zh菙n)宸ヤ綔娑�:鍒嗗垾鍚稿彇0.5mL銆�1.0mL銆�2.0mL銆�4.0mL銆�5.0mL鐢查唶妯�(bi膩o)婧�(zh菙n)鍎�(ch菙)鍌欐恫,浜�5鍊�(g猫)25mL瀹归噺鐡朵腑,鐢ㄤ箼閱囨憾娑插畾瀹硅嚦鍒诲害,渚濇閰嶅埗鎴愮敳閱囧惈閲忕偤100mg/L銆�200mg/L銆�400mg/L銆�
800mg/L銆�1000mg/L绯诲垪妯�(bi膩o)婧�(zh菙n)婧舵恫,鐝�(xi脿n)閰嶇従(xi脿n)鐢�銆�
鍥�銆佺櫧閰掍腑鐢查唶妾㈡脯(c猫)鍎€鍣ㄥ垎鏋愭椹�
1銆佽│妯ｅ墠铏曠悊
鍚稿彇100mL瑭︽ǎ浜�500mL钂搁ぞ鐡朵腑,骞跺姞鍏�100mL姘�,鍔犲咕椤嗘哺鐭�(鎴栫幓鐠冪彔),閫ｆ帴鍐峰嚌绠�,
鐢�100mL瀹归噺鐡朵綔鐐烘帴鏀跺櫒(澶栧姞鍐版荡),骞堕枊(k膩i)鍟熷喎鍗绘按,绶╂參鍔犵啽钂搁ぞ,鏀堕泦椁惧嚭娑�,鐣�(d膩ng)鎺ヨ繎鍒诲害鏅�(sh铆),
鍙栦笅瀹归噺鐡�,寰呮憾娑插喎鍗诲埌瀹ゆ韩鍚�,鐢ㄦ按瀹氬鑷冲埢搴�,娣峰嫽銆傚惛鍙�10.0mL钂搁ぞ鍚庣殑婧舵恫浜庤│绠′腑,鍔�
鍏�0.10mL鍙旀垔閱囨(bi膩o)婧�(zh菙n)婧舵恫,娣峰嫽,鍌欑敤銆�
2銆侀厭绮俱€佽捀椁鹃厭鍙婂叾閰嶅埗閰�
鍚稿彇瑭︽ǎ10.0mL浜庤│绠′腑,鍔犲叆0.10mL鍙旀垔閱囨(bi膩o)婧�(zh菙n)婧舵恫,娣峰嫽,鍌欑敤;鐣�(d膩ng)瑭︽ǎ椤忚壊杓冩繁,鎸夌収
3銆佹埃鐩歌壊璀滃剙鎿嶄綔姊濅欢
a) 鑹茶瓬鏌�:鑱氫箼浜岄唶鐭宠嫳姣涚窗(x矛)绠℃煴,鏌遍暦(zh菐ng)60m,鍏�(n猫i)寰�0.25mm,鑶滃帤0.25渭m,鎴栫瓑鏁堟煴;
b) 鑹茶瓬鏌辨韩搴�:鍒濇韩40鈩�,淇濇寔1min,浠�4.0鈩�/min鍗囧埌130鈩�,浠�20鈩�/min鍗囧埌200鈩�,淇�
鎸�5min;
c) 妾㈡脯(c猫)鍣ㄦ韩搴�:250鈩�;
d) 閫�(j矛n)妯ｅ彛婧害:250鈩�;
e) 杓夋埃娴侀噺:1.0mL/min;
f) 閫�(j矛n)妯ｉ噺:1.0渭L;
g) 鍒嗘祦姣�:20鈭�1銆�
4銆佹(bi膩o)婧�(zh菙n)鏇茬窔鐨勫埗浣�
鍒嗗垾鍚稿彇10mL鐢查唶绯诲垪妯�(bi膩o)婧�(zh菙n)宸ヤ綔娑蹭簬5鍊�(g猫)瑭︾涓�,鐒跺悗鍔犲叆0.10mL鍙旀垔閱囨(bi膩o)婧�(zh菙n)婧舵恫,娣峰嫽,娓�(c猫)
瀹氱敳閱囧拰鍏�(n猫i)妯�(bi膩o)鍙旀垔閱囪壊璀滃嘲闈㈢⿳,浠ョ敳閱囩郴鍒楁(bi膩o)婧�(zh菙n)宸ヤ綔娑茬殑婵冨害鐐烘┇鍧愭(bi膩o),浠ョ敳閱囧拰鍙旀垔閱囪壊璀滃嘲闈㈢⿳
鐨勬瘮鍊肩偤绺卞潗妯�(bi膩o),绻埗妯�(bi膩o)婧�(zh菙n)鏇茬窔(鐢查唶鍙婂収(n猫i)妯�(bi膩o)鍙旀垔閱囨(bi膩o)婧�(zh菙n)鐨勬埃鐩歌壊璀滃湒瑕�(ji脿n)鍦朅.1)銆�
5銆佽│妯ｆ憾娑茬殑娓�(c猫)瀹�
灏囧埗鍌欑殑瑭︽ǎ婧舵恫娉ㄥ叆姘ｇ浉鑹茶瓬鍎€涓�,浠ヤ繚鐣欐檪(sh铆)闁撳畾鎬�,鍚屾檪(sh铆)瑷橀寗鐢查唶鍜屽彅鎴婇唶鑹茶瓬宄伴潰绌嶇殑姣�
鍊�,鏍规摎(j霉)妯�(bi膩o)婧�(zh菙n)鏇茬窔鎿佹湁寰呮脯(c猫)娑蹭腑鐢查唶鐨勬績搴�銆�
6銆佹娓�(c猫)鑼冨湇
鏂规硶妾㈠嚭闄愮偤7.5mg/L,瀹氶噺闄愮偤25mg/L銆�
鍞悗鏈嶅嫏(w霉)鎵胯
淇濅慨鏈�: 1骞�
鏄惁鍙欢闀�(zh菐ng)淇濅慨鏈�: 鍚�
鐝�(xi脿n)鍫�(ch菐ng)鎶€琛�(sh霉)鍜ㄨ: 鏈�
鍏嶈不(f猫i)鍩硅〒(x霉n): 鍏嶈不(f猫i)鍩硅〒(x霉n)
鍏嶈不(f猫i)鍎€鍣ㄤ繚椁�(y菐ng): 涓€骞村収(n猫i)鍏嶈不(f猫i)
淇濆収(n猫i)缍慨鎵胯: 8灏忔檪(sh铆)鍏�(n猫i)鍥炲京(f霉)
鍫�(b脿o)淇壙璜�: 72灏忔檪(sh铆)鍏�(n猫i)鍥炲京(f霉)
