涓€銆佺櫧閰掍腑鐢查唶妾㈡脯鍒嗘瀽鍘熺悊锛�
鎸夌収銆婇鍝佷腑鐢查唶鐨勬脯瀹氥€嬭捀椁鹃櫎鍘荤櫦(f膩)閰甸厭鍙婂叾閰嶅埗閰掍腑涓嶆彯鐧�(f膩)鎬х墿璩�(zh矛),鍔犲叆鍏�(n猫i)妯�(閰掔簿銆佽捀椁鹃厭鍙婂叾閰嶅埗閰掔洿鎺ュ姞鍏ュ収(n猫i)妯�),缍�(j墨ng)姘ｇ浉鑹茶瓬鍎€鑹茶瓬鏌卞垎闆�,姘伀鐒伴洟瀛愬寲妾㈡脯鍣ㄦ娓�,浠ヤ繚鐣欐檪闁撳畾鎬�,鍏�(n猫i)妯欐硶瀹氶噺
浜�銆佺櫧閰掍腑鐢查唶妾㈡脯鍎€鍣ㄥ強妯欐簴鍝�
GC-9860姘ｇ浉鑹茶瓬鍎€锛團ID姘伀鐒版娓櫒+姣涚窗绠＄郴绲�(t菕ng)+鍏礆绋嬪崌锛� 1鑷�
鐧介厭鍒嗘瀽灏堢敤鏌憋紙PEG姣涚窗绠℃煴60绫筹級 1鏀�
鑹茶瓬宸ヤ綔绔� 1濂�
绌烘埃銆佹爱姘�銆佹矮姘ｇ櫦(f膩)鐢熷櫒鎴栭嫾鐡� 1濂�1路 1
闆昏叇鎵撳嵃姗熻嚜閰� 1鑷�
妯欐簴鍝�
涔欓唶婧舵恫(40%,楂旂⿳鍒嗘暩(sh霉)):閲忓彇40mL涔欓唶,鐢ㄦ按瀹氬鑷�100mL,娣峰嫽銆�
鐢查唶(CH4O,CAS铏�:67-56-1):绱斿害鈮�99%?锛涜毆?j墨ng)鍦嬪瑾嶈瓑骞舵巿浜堟婧栫墿璩�(zh矛)璀夋浉鐨勬婧栫墿璩�(zh矛)銆�
鍙旀垔閱�(C5H12O,CAS铏�:75-85-4):绱斿害鈮�99%銆�
涓�銆佺櫧閰掍腑鐢查唶妾㈡脯鍎€鍣ㄦ婧栨憾娑查厤鍒�
鐢查唶妯欐簴鍎插倷娑�(5000mg/L):婧栫⒑绋卞彇0.5g(**鑷�0.001g)鐢查唶鑷�100mL瀹归噺鐡朵腑,鐢ㄤ箼閱囨憾娑插畾瀹硅嚦鍒诲害,娣峰嫽,0鈩儈4鈩冧綆婧啺绠卞瘑灏佷繚瀛�銆�
鍙旀垔閱囨婧栨憾娑�(20000mg/L):婧栫⒑绋卞彇2.0g(**鑷�0.001g)鍙旀垔閱囪嚦100mL瀹归噺鐡朵腑,鐢ㄤ箼閱囨憾娑插畾瀹硅嚦100mL,娣峰嫽,0鈩儈4鈩冧綆婧啺绠卞瘑灏佷繚瀛�銆�
鐢查唶绯诲垪妯欐簴宸ヤ綔娑�:鍒嗗垾鍚稿彇0.5mL銆�1.0mL銆�2.0mL銆�4.0mL銆�5.0mL鐢查唶妯欐簴鍎插倷娑�,浜�5鍊�25mL瀹归噺鐡朵腑,鐢ㄤ箼閱囨憾娑插畾瀹硅嚦鍒诲害,渚濇閰嶅埗鎴愮敳閱囧惈閲忕偤100mg/L銆�200mg/L銆�400mg/L銆�
800mg/L銆�1000mg/L绯诲垪妯欐簴婧舵恫,鐝�(xi脿n)閰嶇従(xi脿n)鐢ㄣ€�
鍥�銆佺櫧閰掍腑鐢查唶妾㈡脯鍎€鍣ㄥ垎鏋愭椹�
1銆佽│妯ｅ墠铏曠悊
鍚稿彇100mL瑭︽ǎ浜�500mL钂搁ぞ鐡朵腑,骞跺姞鍏�100mL姘�,鍔犲咕椤嗘哺鐭�(鎴栫幓鐠冪彔),閫ｆ帴鍐峰嚌绠�,
鐢�100mL瀹归噺鐡朵綔鐐烘帴鏀跺櫒(澶栧姞鍐版荡),骞堕枊鍟熷喎鍗绘按,绶╂參鍔犵啽钂搁ぞ,鏀堕泦椁惧嚭娑�,鐣舵帴杩戝埢搴︽檪,
鍙栦笅瀹归噺鐡�,寰呮憾娑插喎鍗诲埌瀹ゆ韩鍚�,鐢ㄦ按瀹氬鑷冲埢搴�,娣峰嫽銆傚惛鍙�10.0mL钂搁ぞ鍚庣殑婧舵恫浜庤│绠′腑,鍔�
鍏�0.10mL鍙旀垔閱囨婧栨憾娑�,娣峰嫽,鍌欑敤銆�
2銆侀厭绮�銆佽捀椁鹃厭鍙婂叾閰嶅埗閰�
鍚稿彇瑭︽ǎ10.0mL浜庤│绠′腑,鍔犲叆0.10mL鍙旀垔閱囨婧栨憾娑�,娣峰嫽,鍌欑敤;鐣惰│妯ｉ鑹茶純娣�,鎸夌収
3銆佹埃鐩歌壊璀滃剙鎿嶄綔姊濅欢
a) 鑹茶瓬鏌�:鑱氫箼浜岄唶鐭宠嫳姣涚窗绠℃煴,鏌遍暦60m,鍏�(n猫i)寰�0.25mm,鑶滃帤0.25渭m,鎴栫瓑鏁堟煴;
b) 鑹茶瓬鏌辨韩搴�:鍒濇韩40鈩�,淇濇寔1min,浠�4.0鈩�/min鍗囧埌130鈩�,浠�20鈩�/min鍗囧埌200鈩�,淇�
鎸�5min;
c) 妾㈡脯鍣ㄦ韩搴�:250鈩�;
d) 閫叉ǎ鍙ｆ韩搴�:250鈩�;
e) 杓夋埃娴侀噺:1.0mL/min;
f) 閫叉ǎ閲�:1.0渭L;
g) 鍒嗘祦姣�:20鈭�1銆�
4銆佹婧栨洸绶氱殑鍒朵綔
鍒嗗垾鍚稿彇10mL鐢查唶绯诲垪妯欐簴宸ヤ綔娑蹭簬5鍊嬭│绠′腑,鐒跺悗鍔犲叆0.10mL鍙旀垔閱囨婧栨憾娑�,娣峰嫽,娓�
瀹氱敳閱囧拰鍏�(n猫i)妯欏彅鎴婇唶鑹茶瓬宄伴潰绌�,浠ョ敳閱囩郴鍒楁婧栧伐浣滄恫鐨勬績搴︾偤姗潗妯�,浠ョ敳閱囧拰鍙旀垔閱囪壊璀滃嘲闈㈢⿳
鐨勬瘮鍊肩偤绺卞潗妯�,绻埗妯欐簴鏇茬窔(鐢查唶鍙婂収(n猫i)妯欏彅鎴婇唶妯欐簴鐨勬埃鐩歌壊璀滃湒瑕嬪湒A.1)銆�
5銆佽│妯ｆ憾娑茬殑娓畾
灏囧埗鍌欑殑瑭︽ǎ婧舵恫娉ㄥ叆姘ｇ浉鑹茶瓬鍎€涓�,浠ヤ繚鐣欐檪闁撳畾鎬�,鍚屾檪瑷橀寗鐢查唶鍜屽彅鎴婇唶鑹茶瓬宄伴潰绌嶇殑姣�
鍊�,鏍规摎(j霉)妯欐簴鏇茬窔鎿佹湁寰呮脯娑蹭腑鐢查唶鐨勬績搴�銆�
6銆佹娓寖鍦�
鏂规硶妾㈠嚭闄愮偤7.5mg/L,瀹氶噺闄愮偤25mg/L銆�
鍞悗鏈嶅嫏(w霉)鎵胯
淇濅慨鏈�: 1骞�
鏄惁鍙欢闀蜂繚淇湡: 鍚�
鐝�(xi脿n)鍫存妧琛�(sh霉)鍜ㄨ: 鏈�
鍏嶈不鍩硅〒(x霉n): 鍏嶈不鍩硅〒(x霉n)
鍏嶈不鍎€鍣ㄤ繚椁�(y菐ng): 涓€骞村収(n猫i)鍏嶈不
淇濆収(n猫i)缍慨鎵胯: 8灏忔檪鍏�(n猫i)鍥炲京(f霉)
鍫变慨鎵胯: 72灏忔檪鍏�(n猫i)鍥炲京(f霉)
